DP105-CLEAR

Page 1 of 11 3M™ Scotch-Weld™ Epoxy Adhesive DP105 Clear Last Revision Date: October, 2017 Product Description 3M™ Scotch-Weld™ Epoxy Adhesive DP105 Clear is available in larger containers like 3M™ Scotch-Weld™ Epoxy Adhesive 105 B/A Clear. 3M™ Scotch-Weld Epoxy Adhesive DP105 Clear is a fast setting, very flexible 1:1 mix ratio epoxy adhesive/sealant. Its flexibility when cured makes it ideal for applications involving dissimilar surfaces where thermal coefficient of expansion may be a problem. It is also unique in that it retains its clear, colorless properties longer than most 5 minute epoxies. Product Features • 4 minute worklife • High peel strength • Flexible • 1:1 mix ratio • Clear Technical Information Note The following technical information and data should be considered representative or typical only and should not be used for specification purposes. Typical Uncured Physical Properties Property Values Color Clear Additional Information View Notes: Colors may vary from nearly white to yellow/amber. Adhesive performance is not affected by color variation. Base Color Clear Accelerator Color Clear Base Viscosity 1,000-5,000 cP View Test Method: 3M C1d Temp C: 27C Temp F: 80F Notes: Procedure involves Brookfield RVF, #7 spindle, 20 rpm. Measurement taken after 1 minute rotation. Accelerator Viscosity Test Method: 3M C1d Temp C: 27C 8,000-16,000 cP View Page 2 of 11 Temp F: 80F Notes: Procedure involves Brookfield RVF, #7 spindle, 20 rpm. Measurement taken after 1 minute rotation. Base Resin Epoxy Accelerator Resin Mercaptan Base Net Weight 9.1 to 9.5 lb/gal Accelerator Net Weight 9.4 to 9.8 lb/gal Mix Ratio by Volume (B:A) 1:1 Mix Ratio by Weight (B:A) 1:0.97 Typical Mixed Physical Properties Property Values Additional Information Open Time 5 min View 37 °C (98 °F, 110 °C, 230 °F) View Notes: POR=Pop Off Rubber Exotherm max temp Notes: Exotherm determined using the stated mass mixed for 1 minute and then by electronic thermocouple measuring the peak temperature and time to that temperature. Exotherm max temp 98 °F View Notes: Exotherm determined using the stated mass mixed for 1 minute and then by electronic thermocouple measuring the peak temperature and time to that temperature. Exotherm time to reach max temp 5 min (3 min) View Notes: Exotherm determined using the stated mass mixed for 1 minute and then by electronic thermocouple measuring the peak temperature and time to that temperature. Exotherm max temp 110 °C View Notes: Exotherm determined using the stated mass mixed for 1 minute and then by electronic thermocouple measuring the peak temperature and time to that temperature. Exotherm max temp 230 °F View Page 3 of 11 Notes: Exotherm determined using the stated mass mixed for 1 minute and then by electronic thermocouple measuring the peak temperature and time to that temperature. Exotherm time to reach max temp 3 min View Notes: Exotherm determined using the stated mass mixed for 1 minute and then by electronic thermocouple measuring the peak temperature and time to that temperature. Worklife, 2g mixed 5 min View Test Method: 3M C3180 Temp C: 23C Temp F: 73F Notes: Procedure involves periodically measuring a 2 gram mixed mass for self leveling and wetting properties. This time will also approximate the usable worklife in an 3M™ EPX™ Applicator mixing nozzle. Worklife, 20g mixed 4 min View Test Method: 3M C3180 Temp C: 23C Temp F: 73F Notes: Procedure involves periodically measuring a 2 gram mixed mass for self leveling and wetting properties. This time will also approximate the usable worklife in an 3M™ EPX™ Applicator mixing nozzle. Worklife 3 to 4 min View Test Method: 3M C3180 Temp C: 23C Temp F: 73F Notes: Procedure involves periodically measuring a 2 gram mixed mass for self leveling and wetting properties. This time will also approximate the usable worklife in an 3M™ EPX™ Applicator mixing nozzle. Time to Handling Strength 20 min View Temp C: 23C Temp F: 73F Notes: Minimum time required to achieve 50 psi of overlap shear strength. Cure times are approximate and depend on adhesive temperature. Tack Free Time 10 min View Test Method: 3M C3173 Notes: Involves dispensing 0.5 gram amount of adhesive onto substrate and testing periodically for no adhesive transfer to metal spatula. Time to Full Cure 0.33 hr View Temp C: 23C Temp F: 73F Notes: The cure time is defined as that time required for the adhesive to achieve a minimum of 80% of the ultimate strength as measured by aluminum-aluminum OLS. Time to Full Cure 48 hr View 250 lb/in² View Temp C: 23C Temp F: 73F Rate of Strength Buildup 1hr Page 4 of 11 Test Method: ASTM D1002 Test Name: Overlap Shear Strength Dwell/Cure Time: 1.0 Dwell Time Units: hr Temp C: 23C Temp F: 72F Substrate: Etched Aluminum Notes: 1 in wide 1/2 in overlap specimens with 1 in x 4 in substrates. 0.005-0.008in bondline. Jaw separation 0.1 in/min. Substrate thickness 0.05-0.064 in Rate of Strength Buildup 6hr 500 lb/in² View Test Method: ASTM D1002 Test Name: Overlap Shear Strength Dwell/Cure Time: 6.0 Dwell Time Units: hr Temp C: 23C Temp F: 72F Substrate: Etched Aluminum Notes: 1 in wide 1/2 in overlap specimens with 1 in x 4 in substrates. 0.005-0.008in bondline. Jaw separation 0.1 in/min. Substrate thickness 0.05-0.064 in Rate of Strength Buildup 1day 1000 lb/in² View Test Method: ASTM D1002 Test Name: Overlap Shear Strength Dwell/Cure Time: 1.0 Dwell Time Units: day Temp C: 23C Temp F: 72F Substrate: Etched Aluminum Notes: 1 in wide 1/2 in overlap specimens with 1 in x 4 in substrates. 0.005-0.008in bondline. Jaw separation 0.1 in/min. Substrate thickness 0.05-0.064 in Rate of Strength Buildup 7day 2000 lb/in² View Test Method: ASTM D1002 Test Name: Overlap Shear Strength Dwell/Cure Time: 7.0 Dwell Time Units: day Temp C: 23C Temp F: 72F Substrate: Etched Aluminum Notes: 1 in wide 1/2 in overlap specimens with 1 in x 4 in substrates. 0.005-0.008in bondline. Jaw separation 0.1 in/min. Substrate thickness 0.05-0.064 in Rate of Strength Buildup 1month 2000 lb/in² View Test Method: ASTM D1002 Test Name: Overlap Shear Strength Dwell/Cure Time: 1.0 Dwell Time Units: month Temp C: 23C Temp F: 72F Substrate: Etched Aluminum Notes: 1 in wide 1/2 in overlap specimens with 1 in x 4 in substrates. 0.005-0.008in bondline. Jaw separation 0.1 in/min. Substrate thickness 0.05-0.064 in Typical Physical Properties Property Values Color Clear Test Name: Cured Additional Information View Page 5 of 11 Typical Cured Characteristics Property Values Additional Information Shore D Hardness 27 View 600 lb/in² View Test Method: ASTM D2240 Temp C: 23C Temp F: 73F Tensile Strength Test Method: ASTM D882 Dwell/Cure Time: 2.0 Dwell Time Units: hr Temp C: 23C Temp F: 72F Environmental Condition: +2 hr @ 160F(71C) Notes: Samples were 2 in. dumbbells with 0.125 in. neck and .030 in. sample thickness. Separation rate was 2 inches per minute. Weight Loss by Thermal Gravimetric Analysis (TGA) 1% View Test Method: ASTM E1131 Temp C: 117C Temp F: 243F Notes: Weight loss by Thermal Gravimetric Analysis reported as that temperature at which 5% weight loss occurs by TGA in air at 5°C (9°F) rise per minute. Thermal Shock Resistance Pass 5 cycles without cracking View Test Method: 3M C3174 Notes: Involves potting a metal washer into a 2 in. x 0.5 in. thick section and cycling this test specimen to colder and colder temperatures. Weight Loss by Thermal Gravimetric Analysis (TGA) 289 °C (552 F) View Test Method: ASTM E1131 Notes: Weight loss by Thermal Gravimetric Analysis reported as that temperature at which 5% weight loss occurs by TGA in air at 5°C (9°F) rise per minute. Weight Loss by Thermal Gravimetric Analysis (TGA) 552 F View Test Method: ASTM E1131 Notes: Weight loss by Thermal Gravimetric Analysis reported as that temperature at which 5% weight loss occurs by TGA in air at 5°C (9°F) rise per minute. Typical Performance Characteristics Property Values Elongation 120 % Test Method: ASTM D882 Dwell/Cure Time: 2.0 Dwell Time Units: hr Temp C: 23C Temp F: 72F Environmental Condition: +2 hr @ 160F(71C) Additional Information View Page 6 of 11 Notes: Samples were 2 in. dumbbells with 0.125 in. neck and .030 in. sample thickness. Separation rate was 2 inches per minute. T-Peel Adhesion -55C Etched Aluminum 3 lb/in width View Test Method: ASTM D1876 Test Name: T-Peel Adhesion Temp C: -55C Temp F: -67F Substrate: Etched Aluminum Notes: T-peel strengths were measured on 1 in. wide bonds at 73°F (23°C). The testing jaw separation rate was 20 inches per minute. The substrates were 0.020 in. thick. Samples dwelled for 24 hrs at 23C + 2 hrs at 71C before testing. T-Peel Adhesion 23C Etched Aluminum 35 lb/in width View Test Method: ASTM D1876 Test Name: T-Peel Adhesion Temp C: 23C Temp F: 73F Substrate: Etched Aluminum Notes: T-peel strengths were measured on 1 in. wide bonds at 73°F (23°C). The testing jaw separation rate was 20 inches per minute. The substrates were 0.020 in. thick. Samples dwelled for 24 hrs at 23C + 2 hrs at 71C before testing. T-Peel Adhesion 49C Etched Aluminum 5 lb/in width View Test Method: ASTM D1876 Test Name: T-Peel Adhesion Temp C: 49C Temp F: 120F Substrate: Etched Aluminum Notes: T-peel strengths were measured on 1 in. wide bonds at 73°F (23°C). The testing jaw separation rate was 20 inches per minute. The substrates were 0.020 in. thick. Samples dwelled for 24 hrs at 23C + 2 hrs at 71C before testing. T-Peel Adhesion 66C Etched Aluminum 2 lb/in width View Test Method: ASTM D1876 Test Name: T-Peel Adhesion Temp C: 66C Temp F: 150F Substrate: Etched Aluminum Notes: T-peel strengths were measured on 1 in. wide bonds at 73°F (23°C). The testing jaw separation rate was 20 inches per minute. The substrates were 0.020 in. thick. Samples dwelled for 24 hrs at 23C + 2 hrs at 71C before testing. T-Peel Adhesion 82C Etched Aluminum 1 lb/in width View Test Method: ASTM D1876 Test Name: T-Peel Adhesion Temp C: 82C Temp F: 180F Substrate: Etched Aluminum Notes: T-peel strengths were measured on 1 in. wide bonds at 73°F (23°C). The testing jaw separation rate was 20 inches per minute. The substrates were 0.020 in. thick. Samples dwelled for 24 hrs at 23C + 2 hrs at 71C before testing. Solvent Resistance Acetone 1hr A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Acetone 1hr Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance Acetone 1month A Page 7 of 11 View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Acetone 1mo Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance Isopropyl Alcohol 1hr A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Isopropyl Alcohol 1hr Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance Isopropyl Alcohol 1month A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Isopropyl Alcohol 1mo Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance Freon TF 1hr A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Freon TF 1hr Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance Freon TF 1month A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Freon TF 1mo Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance Freon TMC 1hr A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Freon TMC 1hr Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance Freon TMC 1month B View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + Freon TMC 1mo Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance 1, 1, 1 - Trichloroethane 1hour A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + 1, 1, 1 - Trichloroethane 1hr Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance 1, 1, 1 - Trichloroethane 1month A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + 1, 1, 1 - Trichloroethane 1mo Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance RMA Flux 1hr A View Page 8 of 11 Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + RMA Flux 1hr Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Solvent Resistance RMA Flux 1month A View Environmental Condition: 24hr @ RT + 2hr @ 160F(71C) + RMA Flux 1mo Notes: Cured OLS samples immersed in solvent and after dwell, examined for surface attack compared to control. A: Unaffected, no color or texture change B: Slight attack, slight swelling of surface. C: Moderate/severe attack, extreme swelling of surface. Electrical and Thermal Properties Property Values Glass Transition Temperature (Tg) 15 °C (59 °F, 8 °C, 46 °F) Additional Information View Notes: Glass Transition Temperature (Tg) determined using DSC Analyzer with a heating rate of 68°F (20°C) per minute. Second heat values given. Glass Transition Temperature (Tg) 59 °F View Notes: Glass Transition Temperature (Tg) determined using DSC Analyzer with a heating rate of 68°F (20°C) per minute. Second heat values given. Glass Transition Temperature (Tg) 8 °C View Notes: Glass Transition Temperature (Tg) determined using DSC Analyzer with a heating rate of 68°F (20°C) per minute. Second heat values given. Glass Transition Temperature (Tg) 46 °F View Notes: Glass Transition Temperature (Tg) determined using DSC Analyzer with a heating rate of 68°F (20°C) per minute. Second heat values given. Dielectric Constant 1KHz 9.2 View 0.22 View 0.35 x 10^-3 Cal/s/cm/°C (14.7 W/m/K, 0.085 View Test Method: ASTM D150 Temp C: 23C Temp F: 72F Dissipation Factor 1KHz Test Method: ASTM D150 Temp C: 23C Temp F: 72F Thermal Conductivity (btu-ft)/(h-ft²-°F)) Test Method: C177 Temp F: 110F Notes: Thermal conductivity determined using C-matic Instrument using 2 in. diameter samples. Thermal Conductivity Test Method: C177 14.7 W/m/K View Page 9 of 11 Temp F: 110F Notes: Thermal conductivity determined using C-matic Instrument using 2 in. diameter samples. Thermal Conductivity 0.085 (btu-ft)/(h-ft²-°F) View Test Method: C177 Temp F: 110F Notes: Thermal conductivity determined using C-matic Instrument using 2 in. diameter samples. Volume Resistivity 1.5 x 10^10 Ω-cm View 181 x 10^-6 m/m/°C View Test Method: ASTM D257 Temp C: 23C Temp F: 73F Coefficient of Thermal Expansion Notes: TCE determined using TMA Analyzer using a heating rate of 10°C per minute. Second heat values given. Storage and Shelf Life Store 3M™ Scotch-Weld™ Epoxy Adhesive DP-105 Clear at 60-80°F (15-27°C) for maximum shelf life. These epoxy adhesive products have a shelf life of 24 months in their unopened bulk containers. Shelf life is determined from the date of manufacture. Industry Specifications EN 45545 test report for details (ISO 5659-2, ISO 9239-1, ISO 5660-1, ISO 5658-2) Bottom Matter 3M Industrial Adhesives and Tapes Division 3M Center, Building 225-3S-06 St. Paul, MN 55144-1000 800-362-3550 • 877-369-2923 (Fax) www.3M.com Trademarks 3M, Scotch-Weld, Novec and EPX are trademarks of 3M Company. Handling/Application Information Directions for Use 1. For high strength structural bonds, paint, oxide films, oils, dust, mold release agents and all other surface contaminants must be completely removed. However, the amount of surface preparation directly depends on the required bond strength and the environmental aging resistance desired by user. For specific surface preparations on common substrates, see the following section on Surface Preparation. 2. Uses gloves to minimize skin contact. Do not use solvents for cleaning hands. 3. Mixing For Duo-Pak Cartridges 3M™ Scotch-Weld™ Epoxy Adhesive DP105 Clear is supplied in a dual syringe plastic Duo-Pak cartridge as part of the 3M™ Scotch-Weld™ EPX™ Applicator system. To use, simply insert the Duo-Pak cartridge into the EPX applicator and start the plunger into the cylinders using light pressure on the trigger. Next, remove the Duo-Pak cartridge cap and expel a small amount of adhesive to be sure both sides of the Duo-Pak cartridge are flowing evenly and freely. If automatic mixing of Part A and Part B is desired, attach the EPX mixing nozzle to the Duo- Pak cartridge and begin dispensing the adhesives. For hand mixing, expel the desired amount of adhesive and mix thoroughly. Mix approximately 15 seconds after uniform color is obtained. Page 10 of 11 For Bulk Containers Mix thoroughly by weight or volume in the proportions specified in the Typical Uncured Properties section. Mix approximately 15 seconds after uniform color is obtained. 4. For maximum bond strength apply adhesive evenly to both surfaces to be joined. 5. Application to the substrates should be made within 3 minutes. Larger quantities and/or higher temperatures will reduce this working time. 6. Join the adhesive coated surfaces and allow to cure at 60°F (16°C) or above until completely firm. Heat up to 200°F (93°C), will speed curing. These products will cure in 48 hours @ 75°F (24°C). 7. Keep parts from moving during cure. Contact pressure is necessary. Maximum shear strength is obtained with a 3-5 mil bond line. 8. Excess uncured adhesive can be cleaned up with ketone type solvents.* Adhesive Coverage: A 0.005 in. thick bondline will yield a coverage of 320 sqft/ gallon. *Note: When using solvents, extinguish all ignition sources and follow the manufacturer’s precautions and directions for use. Surface Preparation For high strength structural bonds, paint, oxide films, oils, dust, mold release agents and all other surface contaminants must be completely removed. However, the amount of surface preparation directly depends on the required bond strength and the environmental aging resistance desired by the user. The following cleaning methods are suggested for common surfaces: Steel: 1. Wipe free of dust with oil-free solvent such as acetone, isopropyl or alcohol solvents.* 2. Sandblast or abrade using clean fine grit abrasives. 3. Wipe again with solvent to remove loose particles. 4. If a primer is used, it should be applied within 4 hours after surface preparation. Aluminum: 1. Vapor Degrease: 3M™ Novec™ condensing vapors for 5-10 minutes. 2. Alkaline Degrease: Oakite 164 solution (9-11 oz./gallon water) at 190°F ± 10°F (88°C ± 5°C) for 10-20 minutes. Rinse immediately in large quantities of cold running water. 3. Acid Etch: Place panels in the following solution for 10 minutes at 150°F ± 5°F (66°C ± 2°C). Sodium Dichromate 4.1 - 4.9 oz./gallon Sulfuric Acid, 66°Be 38.5 - 41.5 oz./gallon 2024-T3 aluminum (dissolved) 0.2 oz./gallon minimum Tap Water as needed to balance 4. Rinse: Rinse panels in clean running tap water. 5. Dry: Air dry 15 minutes; force dry 10 minutes at 150°F ± 10°F (66°C ± 5°C). 6. If primer is to be used, it should be applied within 4 hours after surface preparation. Plastics/Rubber: 1. Wipe with isopropyl alcohol.* 2. Abrade using fine grit abrasives. 3. Wipe with isopropyl alcohol.* Glass: 1. Solvent wipe surface using acetone or MEK.* *Note: When using solvents, extinguish all ignition sources and follow the manufacturer’s precautions and directions for use. • For small or intermittent applications the 3M™ Scotch-Weld™ EPX™ Applicator is a convenient method of application. • For larger applications, these products may be applied by use of flow equipment. • Two part meter/mixing/dispensing equipment is available for intermittent or production line use. These systems may be desirable because of their variable shot size and flow rate characteristics and are adaptable to many applications. Page 11 of 11 References Property Values 3m.com Product Page https://www.3m.com/3M/en_US/company-us/all-3m-products/~/3M-Scotch-Weld-Epoxy-Adhesive-DP105/? N=5002385+3293242301&rt=rud Safety Data Sheet SDS https://www.3m.com/3M/en_US/company-us/SDS-search/results/? gsaAction=msdsSRA&msdsLocale=en_US&co=ptn&q=DP105 Clear Family Group Link Tags: DP105 Clear Time to Handling Products Open Time Color Worklife Time to Full Cure Shore D Hardness 48 hr 27 Strength DP105 Clear 5 min Clear 3 to 4 min 20 min ISO Statement This Industrial Adhesives and Tapes Division product was manufactured under a 3M quality system registered to ISO 9001 standards. Precautionary Information Refer to Product Label and Material Safety Data Sheet for health and safety information before using this product. For additional health and safety information, call 1-800364-3577 or (651) 737-6501. 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